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70 C for 24 h ground for 1 hour in a planetary ball mill MSKSFM1 andmanuallysieved toretainparticles witha sizelower than 106 mm. Batch leaching was conducted in 200 mL plastic bottles under either unstirred or stirred conditions at room temperature. Stirring was controlled using a Corning LSE orbital shaker 6780 NP at 200 rpm.
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